FREE BOOKS

Author's List




PREV.   NEXT  
|<   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41   42   43   44   45  
46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70   >>   >|  
nd until the water is well above the graduation mark. Quickly place the forefinger over the top of the tube, thus preventing the entrance of air and holding the water in the pipette. Cautiously admit a little air by releasing the pressure of the finger, and allow the level of the water to fall until the lowest point of the meniscus is level with the graduation. Hold the water at that point by pressure of the finger and then allow the water to run out from the pipette into a small tared, or weighed, beaker or flask. After a definite time interval, usually two to three minutes, touch the end of the pipette against the side of the beaker or flask to remove any liquid adhering to it (Note 1). The increase in weight of the flask in grams represents the volume of the water in cubic centimeters delivered by the pipette. Calculate the necessary correction. [Note 1: A definite interval must be allowed for draining, and a definite practice adopted with respect to the removal of the liquid which collects at the end of the tube, if the pipette is designed to deliver a specific volume when emptied. This liquid may be removed at the end of a definite interval either by touching the side of the vessel or by gently blowing out the last drops. Either practice, when adopted, must be uniformly adhered to.] FLASKS !Graduated or measuring flasks! are similar to the ordinary flat-bottomed flasks, but are provided with long, narrow necks in order that slight variations in the position of the meniscus with respect to the graduation shall represent a minimum volume of liquid. The flasks must be of such a capacity that, when filled with the specified volume, the liquid rises well into the neck. GRADUATION OF FLASKS It is a general custom to purchase the flasks ungraduated and to graduate them for use under standard conditions selected for the laboratory in question. They may be graduated for "contents" or "delivery." When graduated for "contents" they contain a specified volume when filled to the graduation at a specified temperature, and require to be washed out in order to remove all of the solution from the flask. Flasks graduated for "delivery" will deliver the specified volume of a liquid without rinsing. A flask may, of course, be graduated for both contents and delivery by placing two graduation marks upon it. PROCEDURE.--To calibrate a flask for !contents!, proceed as follows: Clean the flask, using a chromic acid solut
PREV.   NEXT  
|<   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41   42   43   44   45  
46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70   >>   >|  



Top keywords:

volume

 

liquid

 

graduation

 

pipette

 

graduated

 

definite

 

flasks

 

contents

 

delivery

 
interval

beaker
 
respect
 

adopted

 
deliver
 

filled

 
practice
 
remove
 

FLASKS

 

meniscus

 

pressure


finger

 

capacity

 
calibrate
 
proceed
 

GRADUATION

 

chromic

 

bottomed

 

minimum

 

slight

 

provided


narrow

 

variations

 

position

 

represent

 

general

 

purchase

 

rinsing

 
question
 

require

 

washed


solution

 

temperature

 
Flasks
 

placing

 

ungraduated

 

graduate

 
custom
 
PROCEDURE
 

selected

 
laboratory