nd until the water is well above the graduation mark.
Quickly place the forefinger over the top of the tube, thus preventing
the entrance of air and holding the water in the pipette. Cautiously
admit a little air by releasing the pressure of the finger, and allow
the level of the water to fall until the lowest point of the meniscus
is level with the graduation. Hold the water at that point by pressure
of the finger and then allow the water to run out from the pipette
into a small tared, or weighed, beaker or flask. After a definite time
interval, usually two to three minutes, touch the end of the pipette
against the side of the beaker or flask to remove any liquid adhering
to it (Note 1). The increase in weight of the flask in grams
represents the volume of the water in cubic centimeters delivered by
the pipette. Calculate the necessary correction.
[Note 1: A definite interval must be allowed for draining, and a
definite practice adopted with respect to the removal of the liquid
which collects at the end of the tube, if the pipette is designed to
deliver a specific volume when emptied. This liquid may be removed
at the end of a definite interval either by touching the side of the
vessel or by gently blowing out the last drops. Either practice, when
adopted, must be uniformly adhered to.]
FLASKS
!Graduated or measuring flasks! are similar to the ordinary
flat-bottomed flasks, but are provided with long, narrow necks in
order that slight variations in the position of the meniscus with
respect to the graduation shall represent a minimum volume of liquid.
The flasks must be of such a capacity that, when filled with the
specified volume, the liquid rises well into the neck.
GRADUATION OF FLASKS
It is a general custom to purchase the flasks ungraduated and to
graduate them for use under standard conditions selected for the
laboratory in question. They may be graduated for "contents" or
"delivery." When graduated for "contents" they contain a specified
volume when filled to the graduation at a specified temperature, and
require to be washed out in order to remove all of the solution from
the flask. Flasks graduated for "delivery" will deliver the specified
volume of a liquid without rinsing. A flask may, of course, be
graduated for both contents and delivery by placing two graduation
marks upon it.
PROCEDURE.--To calibrate a flask for !contents!, proceed as follows:
Clean the flask, using a chromic acid solut
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