FREE BOOKS

Author's List




PREV.   NEXT  
|<   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   50   51  
52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70   71   72   73   74   75   76   >>   >|  
rough the cork of the bottle. By pressing in the cork into the neck of the bottle, the air within will be compressed, and the liquid will rise in the tube. If now we draw the cork out, with the tube filled with the fluid, and pressing the finger upon the upper orifice, the fluid can be forced out in the smallest quantity, even to a fraction of a drop. 10. _Tin._--This metal is used in the form of foil, cut into strips about half an inch wide. Tin is very susceptible of oxidation, and therefore deprives oxidized substances of their oxygen very quickly, when heated in contact with them. It is employed in blowpipe analysis, for the purpose of producing in glass beads a lower degree of oxidation, particularly if the substance under examination contains only a small portion of such oxide. These oxides give a characteristic color to the bead, and thus are detected. The bead is heated upon charcoal in the reduction flame, with a small portion of the tin, whereby some of the tin is melted and mixes with the bead. The bead should be reduced quickly in the reduction flame, for by continuing the blast too great a while, the oxide of tin separates the other oxides in the reduced or metallic state, while we only require that they shall only be converted into a sub-oxide, in order that its peculiar color may be recognized in the bead. The addition of too much tin causes the bead to present an unclean appearance, and prevents the required reaction. 11. _Silica_ (SiO^{3}).--This acid does not even expel carbonic acid in the wet way, but in a glowing heat it expels the strongest volatile acids. In blowpipe analysis, we use it fused with carbonate of soda to a bead, as a test for sulphuric acid, and in some cases for phosphoric acid. Also with carbonate of soda and borax, for the purpose of separating tin from copper. Finely powdered quartz will answer these purposes. If it cannot be procured, take well washed white sand and mix it with two parts of carbonate of soda and two parts of carbonate of potassa. Melt the materials together, pound up the cooled mass, dissolve in hot water, filter, add to the filtrate hydrochloric acid, and evaporate to dryness. Moisten the dry residue with hydrochloric acid, and boil in water. The silica remains insoluble. It should be washed well, dried, and heated, and then reduced to powder. 12. TEST-PAPERS.--(_a._) _Blue, Litmus Paper._--Dissolve one part of litmus in six or eight parts of wat
PREV.   NEXT  
|<   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   50   51  
52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70   71   72   73   74   75   76   >>   >|  



Top keywords:

carbonate

 

reduced

 
heated
 

quickly

 

oxidation

 
portion
 

analysis

 

blowpipe

 

purpose

 

washed


hydrochloric
 

reduction

 
oxides
 

bottle

 

pressing

 

Finely

 

carbonic

 
powdered
 

quartz

 

copper


separating

 
answer
 

procured

 

purposes

 

phosphoric

 
volatile
 

liquid

 
expels
 
strongest
 

compressed


sulphuric
 

glowing

 

powder

 

insoluble

 

residue

 

silica

 
remains
 

PAPERS

 

litmus

 

Litmus


Dissolve

 

Moisten

 

materials

 
potassa
 
cooled
 

filtrate

 

evaporate

 

dryness

 

filter

 

dissolve