FREE BOOKS

Author's List




PREV.   NEXT  
|<   26   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   50  
51   52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70   71   72   73   74   75   >>   >|  
with this salt, the microscosmic salt is used the same as borax. 9. _Nitrate of Cobalt._--(CoO, NO^{5}).--This salt can be prepared by dissolving pure oxide of cobalt in diluted nitric acid, and evaporating to dryness with a low heat. The dry residue should be dissolved in ten parts of water, and filtered. The filtrate is now ready for use, and should be kept in a bottle with a glass stopper. If the pure oxide of cobalt cannot be procured, then it may be prepared by mixing two parts of finely powdered _glance of cobalt_ with four parts of saltpetre, and one part of dry carbonate of potassa with one part of water free from carbonate of soda. This mixture should be added in successive portions into a red-hot Hessian crucible, and the heat continued until the mass is fused, or at least greatly diminished in volume. The cooled mass must be triturated with hot water, and then heated with hydrochloric acid until it is dissolved and forms a dark green solution, which generally presents a gelatinous appearance, occasioned by separated silica. The solution is to be evaporated to dryness, the dry residue moistened with hydrochloric acid, boiled with water, filtered and neutralized while hot with carbonate of ammonia, until it ceases to give an acid reaction with test-paper. This must now be filtered again, and carbonate of potassa added to the filtrate as long as a precipitate is produced. This precipitate is brought upon a filter and washed thoroughly, and then dissolved in diluted nitric acid. This is evaporated to dryness, and one part of it is dissolved in ten parts of water for use. The oxide of cobalt combines, with strong heat in the oxidation flame, with various earths and infusible metallic oxides, and thus produces peculiarly colored compounds, and is therefore used for their detection; (alumina, magnesia, oxide of zinc, oxide of tin, etc.) Some of the powdered substance is heated upon charcoal in the flame of oxidation, and moistened with a drop of the solution of the nitrate of cobalt, when the oxidation flame is thrown upon it. Alumina gives a pure blue color, the oxide of zinc a bright green, magnesia a light red, and the oxide of tin a bluish-green color; but the latter is only distinctly visible after cooling. The dropping bottle, is the most useful apparatus for the purpose of getting small quantities of fluid. It is composed of a glass tube, drawn out to a point, with a small orifice. This tube passes th
PREV.   NEXT  
|<   26   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   50  
51   52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70   71   72   73   74   75   >>   >|  



Top keywords:

cobalt

 

carbonate

 
dissolved
 

filtered

 

dryness

 
oxidation
 

solution

 

potassa

 

powdered

 

hydrochloric


magnesia
 

evaporated

 
moistened
 

heated

 

precipitate

 

filtrate

 

residue

 
prepared
 

diluted

 

nitric


bottle

 
alumina
 

detection

 

compounds

 

nitrate

 
charcoal
 

substance

 
colored
 
Cobalt
 

Nitrate


strong
 

combines

 

washed

 

earths

 

produces

 

peculiarly

 
oxides
 

infusible

 

metallic

 

passes


apparatus

 

cooling

 

dropping

 
purpose
 
quantities
 

microscosmic

 

filter

 

Alumina

 

composed

 

thrown