FREE BOOKS

Author's List




PREV.   NEXT  
|<   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36   37  
38   39   40   41   42   43   44   45   46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   62   >>   >|  
finity for oxygen, under the influence of the intense heat of that part of the flame. The substance is thus deprived of a part, or the whole, of its oxygen, and becomes _reduced_ according to the strength of the affinity which the substance itself has for oxygen. If the reduction of a substance is undertaken on platinum, by fusion with a flux, and if the oxide is difficult to reduce, the reduction will be completely effected only in the luminous part of the flame. But if a substance be reduced on charcoal, the reduction will take place in the blue part of the flame, as long as the access of air is cut off; but it is the luminous part of the flame which really possesses the greatest reducing power. The following should be observed in order to procure a good reduction flame: The wick should not be too long, that it may make a smoke, nor too short, otherwise the flame will be too small to produce a heat strong enough for reduction. The wick must be free from all loose threads, and from charcoal. The blast should be continued for a considerable time without intermission, otherwise reduction cannot be effected. For the purpose of acquiring practice, the student may fuse the oxide of manganese with borax, upon a platinum wire, in the oxidation flame, when a violet-red glass will be obtained; or if too much of the oxide be used, a glass of a dark color and opaque will be obtained. By submitting this glass to the reduction flame, it will become colorless in correspondence to the perfection with which the flame is produced. Or a piece of tin may be fused upon charcoal, and kept in that state for a considerable time, while it presents the appearance of a bright metal on the surface. This will require dexterity in the operator; for, if the oxidation flame should chance to touch the bright metal only for a moment, it is coated with an infusible oxide. COMBUSTION.--Any flame of sufficient size can be used for blowpipe operations. It may be either the flame of a candle of tallow or wax, or the flame of a lamp. The flame of a wax candle, or of an oil lamp is most generally used. Sometimes a lamp is used filled with a solution of spirits of turpentine in strong alcohol. If a candle is used, it is well to cut the wick off short, and to bend the wick a little toward the substance experimented upon. But candles are not the best for blowpipe operations, as the radiant heat, reflecting from the su
PREV.   NEXT  
|<   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36   37  
38   39   40   41   42   43   44   45   46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   62   >>   >|  



Top keywords:

reduction

 

substance

 
candle
 

oxygen

 

charcoal

 
considerable
 

bright

 

oxidation

 

obtained

 

strong


blowpipe
 

operations

 
reduced
 

effected

 

platinum

 

luminous

 

candles

 
experimented
 

appearance

 

presents


radiant

 
submitting
 

opaque

 

reflecting

 

perfection

 
produced
 

correspondence

 
colorless
 
require
 

filled


sufficient
 

COMBUSTION

 

Sometimes

 

generally

 

tallow

 

infusible

 
solution
 

operator

 

dexterity

 

chance


moment

 

coated

 

spirits

 
turpentine
 
alcohol
 

surface

 

completely

 

reduce

 

difficult

 

access