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7H_{2}O in the presence of sulphuric acid? 6FeSO_{4} + 2HNO_{3} + 3H_{2}SO_{4} = 3Fe_{2}(SO_{4})_{3} + 2NO + 4H_{2}O. !Answer!: 0.80 cc. 81. If 0.7530 gram of ferric nitrate (Fe(NO_{3})_{3}.9H_{2}O) is dissolved in water and 1.37 cc. of HCl (sp. gr. 1.11 containing 21.92% HCl by weight) is added, how many cubic centimeters of ammonia (sp. gr. 0.96 containing 9.91% NH_{3} by weight) are required to neutralize the acid and precipitate the iron as ferric hydroxide? !Answer!: 2.63 cc. 82. To a suspension of 0.3100 gram of Al(OH)_{3} in water are added 13.00 cc. of aqueous ammonia (sp. gr. 0.90 containing 28.4% NH_{3} by weight). How many cubic centimeters of sulphuric acid (sp. gr. 1.18 containing 24.7% H_{2}SO_{4} by weight) must be added to the mixture in order to bring the aluminium into solution? !Answer!: 34.8 cc. 83. How many cubic centimeters of sulphurous acid (sp. gr. 1.04 containing 75 grams SO_{2} per liter) are required to reduce the iron in 1 gram of ferric alum (KFe(SO_{4})_{2}.12H_{2}O)? Fe_{2}(SO_{4})_{3} + SO_{2} + 2H_{2}O = 2FeSO_{4} + 2H_{2}SO_{4}. !Answer!: 0.85 cc. 84. How many cubic centimeters of a solution of potassium bichromate containing 26.30 grams of K_{2}Cr_{2}O_{7} per liter must be taken in order to yield 0.6033 gram of Cr_{2}O_{3} after reduction and precipitation of the chromium? K_{2}Cr_{2}O_{7} + 3SO_{2} + H_{2}SO_{4} = K_{2}SO_{4} + Cr_{2}(SO_{4})_{3} + H_{2}O. !Answer!: 44.39 cc. 85. How many cubic centimeters of ammonium hydroxide (sp. gr. 0.946 containing 13.88% NH_{3} by weight) are required to precipitate the iron as Fe(OH)_{3} from a sample of pure FeSO_{4}.(NH_{4})_{2}SO_{4}.6H_{2}O, which requires 0.34 cc. of nitric acid (sp. gr. 1.350 containing 55.79% HNO_{3} by weight) for oxidation of the iron? (See problem No. 80 for reaction.) !Answer!: 4.74 cc. 86. In the analysis of an iron ore by solution, oxidation and precipitation of the iron as Fe(OH)_{3}, what weight of sample must be taken for analysis so that each one hundredth of a gram of the ignited precipitate of Fe_{2}O_{3} shall represent one tenth of one per cent of iron? !Answer!: 6.99 grams. 87. What weight in grams of impure ferrous ammonium sulphate should be taken for analysis so that the number of centigrams of BaSO_{4} obtained will represent five times the percentage of sulphur in the sample? !Answer!: 0.6870 gram. 88. What weight of magnetite must be taken for analysis in o
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