7H_{2}O in the presence of sulphuric acid? 6FeSO_{4} +
2HNO_{3} + 3H_{2}SO_{4} = 3Fe_{2}(SO_{4})_{3} + 2NO + 4H_{2}O.
!Answer!: 0.80 cc.
81. If 0.7530 gram of ferric nitrate (Fe(NO_{3})_{3}.9H_{2}O) is
dissolved in water and 1.37 cc. of HCl (sp. gr. 1.11 containing 21.92%
HCl by weight) is added, how many cubic centimeters of ammonia (sp.
gr. 0.96 containing 9.91% NH_{3} by weight) are required to neutralize
the acid and precipitate the iron as ferric hydroxide?
!Answer!: 2.63 cc.
82. To a suspension of 0.3100 gram of Al(OH)_{3} in water are added
13.00 cc. of aqueous ammonia (sp. gr. 0.90 containing 28.4% NH_{3} by
weight). How many cubic centimeters of sulphuric acid (sp. gr. 1.18
containing 24.7% H_{2}SO_{4} by weight) must be added to the mixture
in order to bring the aluminium into solution?
!Answer!: 34.8 cc.
83. How many cubic centimeters of sulphurous acid (sp. gr. 1.04
containing 75 grams SO_{2} per liter) are required to reduce the
iron in 1 gram of ferric alum (KFe(SO_{4})_{2}.12H_{2}O)?
Fe_{2}(SO_{4})_{3} + SO_{2} + 2H_{2}O = 2FeSO_{4} + 2H_{2}SO_{4}.
!Answer!: 0.85 cc.
84. How many cubic centimeters of a solution of potassium bichromate
containing 26.30 grams of K_{2}Cr_{2}O_{7} per liter must be taken
in order to yield 0.6033 gram of Cr_{2}O_{3} after reduction and
precipitation of the chromium?
K_{2}Cr_{2}O_{7} + 3SO_{2} + H_{2}SO_{4} = K_{2}SO_{4} +
Cr_{2}(SO_{4})_{3} + H_{2}O.
!Answer!: 44.39 cc.
85. How many cubic centimeters of ammonium hydroxide (sp. gr. 0.946
containing 13.88% NH_{3} by weight) are required to precipitate
the iron as Fe(OH)_{3} from a sample of pure
FeSO_{4}.(NH_{4})_{2}SO_{4}.6H_{2}O, which requires 0.34 cc. of nitric
acid (sp. gr. 1.350 containing 55.79% HNO_{3} by weight) for oxidation
of the iron? (See problem No. 80 for reaction.)
!Answer!: 4.74 cc.
86. In the analysis of an iron ore by solution, oxidation and
precipitation of the iron as Fe(OH)_{3}, what weight of sample must be
taken for analysis so that each one hundredth of a gram of the ignited
precipitate of Fe_{2}O_{3} shall represent one tenth of one per cent
of iron?
!Answer!: 6.99 grams.
87. What weight in grams of impure ferrous ammonium sulphate should
be taken for analysis so that the number of centigrams of BaSO_{4}
obtained will represent five times the percentage of sulphur in the
sample?
!Answer!: 0.6870 gram.
88. What weight of magnetite must be taken for analysis in o
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