FREE BOOKS

Author's List




PREV.   NEXT  
|<   235   236   237   238   239   240   241   242   243   244   245   246   247   248   249   250   251   252   253   254   255   256   257   258   259  
260   261   262   263   264   265   266   267   268   269   270   271   272   273   274   275   276   277   278   279   280   281   282   283   284   >>   >|  
ced, and the hydrogen is disengaged pure in form of gas; in the other case, carbonic acid gas is formed, which disengages, mixed with the hydrogen gas; and this latter is commonly carbonated, or holds charcoal in solution. A musket barrel, without its breach pin, answers exceedingly well for the decomposition of water, by means of iron, and one should be chosen of considerable length, and pretty strong. When too short, so as to run the risk of heating the lute too much, a tube of copper is to be strongly soldered to one end. The barrel is placed in a long furnace, CDEF, Pl. VII. Fig. 11. so as to have a few degrees of inclination from E to F; a glass retort A, is luted to the upper extremity E, which contains water, and is placed upon the furnace VVXX. The lower extremity F is luted to a worm SS, which is connected with the tubulated bottle H, in which any water distilled without decomposition, during the operation, collects, and the disengaged gas is carried by the tube KK to jars in a pneumato-chemical apparatus. Instead of the retort a funnel may be employed, having its lower part shut by a stop-cock, through which the water is allowed to drop gradually into the gun-barrel. Immediately upon getting into contact with the heated part of the iron, the water is converted into steam, and the experiment proceeds in the same manner as if it were furnished in vapours from the retort. In the experiment made by Mr Meusnier and me before a committee of the Academy, we used every precaution to obtain the greatest possible precision in the result of our experiment, having even exhausted all the vessels employed before we began, so that the hydrogen gas obtained might be free from any mixture of azotic gas. The results of that experiment will hereafter be given at large in a particular memoir. In numerous experiments, we are obliged to use tubes of glass, porcelain, or copper, instead of gun-barrels; but glass has the disadvantage of being easily melted and flattened, if the heat be in the smallest degree raised too high; and porcelain is mostly full of small minute pores, through which the gas escapes, especially when compressed by a column of water. For these reasons I procured a tube of brass, which Mr de la Briche got cast and bored out of the solid for me at Strasburg, under his own inspection. This tube is extremely convenient for decomposing alkohol, which resolves into charcoal, carbonic acid gas, and hydrogen gas; it
PREV.   NEXT  
|<   235   236   237   238   239   240   241   242   243   244   245   246   247   248   249   250   251   252   253   254   255   256   257   258   259  
260   261   262   263   264   265   266   267   268   269   270   271   272   273   274   275   276   277   278   279   280   281   282   283   284   >>   >|  



Top keywords:

hydrogen

 

experiment

 

barrel

 

retort

 

copper

 

furnace

 
porcelain
 
extremity
 

employed

 

decomposition


charcoal

 

disengaged

 

carbonic

 

memoir

 

numerous

 

experiments

 

strong

 

obliged

 

disadvantage

 
barrels

results

 

azotic

 

greatest

 

precision

 

result

 

obtain

 

precaution

 

obtained

 
mixture
 

exhausted


vessels

 

easily

 

melted

 

Briche

 

Strasburg

 
convenient
 

decomposing

 

alkohol

 

resolves

 

extremely


inspection

 
procured
 

raised

 

degree

 

flattened

 

smallest

 
minute
 

reasons

 

column

 
compressed