FREE BOOKS

Author's List




PREV.   NEXT  
|<   12   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36  
37   38   39   40   41   42   43   44   45   46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   >>   >|  
excellent account of the properties of glass will be found in Grove's edition of Miller's Elements of Chemistry. Sec. 13. Cleaning Glass Tubes. This is one of the most important arts in chemistry. If the tubes are new, they are generally only soiled by dust, and can be cleaned fairly easily--first by pushing a bit of cotton waste through with a cane, or pulling a rag through with string--and then washing with sand and commercial hydrochloric acid. I have heard of glass becoming scratched by this process, and breaking in consequence when heated, but have never myself experienced this inconvenience. In German laboratories little bits of bibulous paper are sometimes used instead of sand; they soon break into a pulp, and this pulp has a slightly scouring action. As soon as the visible impurities are removed and the tube when washed looks bright and clean, it may be wiped on the outside and held perpendicularly so as to allow the water film to drain down. If the tube be greasy (and perhaps in other cases) it will be observed that as the film gets thinner the water begins to break away and leave dry spots. For accurate work this grease, or whatever it is, must be removed; and after trying many plans for many years, I have come back to the method I first employed, viz. boiling out with aqua regia. For this purpose, close one end of the tube by a cork (better than a rubber bung, because cheaper), and half fill the tube with aqua regia; then, having noted the greasy places, proceed to boil the liquid in contact with the glass at these points, and in the case of very obstinate dirt--such as lingers round a fused joint which has been made between undusted tubes--leave the whole affair for twelve hours. If the greasiness is only slight, then simply shaking with hot aqua regia will often remove it, and the aqua regia is conveniently heated in this case by the addition of a little strong sulphuric acid. The spent aqua regia may be put into a bottle. It is generally quite good enough for the purpose of washing glass vessels with sand, as above explained. However carefully a tube is cleaned before being subjected to blowpipe operations, it will be fouled wherever there is an opening during the process of heating, unless the extreme tip only of an oxidising flame be employed. Even this should not be trusted too implicitly unless an oxygas or hydrogen flame is employed. When a tube or piece of apparatus has been
PREV.   NEXT  
|<   12   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36  
37   38   39   40   41   42   43   44   45   46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   >>   >|  



Top keywords:
employed
 

heated

 

process

 

greasy

 

washing

 

generally

 
removed
 
purpose
 
cleaned
 

lingers


obstinate

 

places

 

rubber

 
cheaper
 

boiling

 

contact

 

points

 

liquid

 

undusted

 

proceed


opening

 

heating

 

extreme

 

fouled

 
subjected
 

blowpipe

 

operations

 

oxidising

 
hydrogen
 

oxygas


apparatus

 

implicitly

 
trusted
 

carefully

 
However
 

remove

 

conveniently

 

addition

 
shaking
 

simply


twelve
 
affair
 

greasiness

 

slight

 

strong

 

sulphuric

 
vessels
 

explained

 

bottle

 

pulling