FREE BOOKS

Author's List




PREV.   NEXT  
|<   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41  
42   43   44   45   46   47   48   49   50   51   52   53   >>  
ation: Fig. 10] _A Spherical Condenser._--Such a condenser as that shown by _f_, Fig 10, involves a method which may find application in a number of cases. The outer bulb is blown from a thick piece of tubing which has been inserted in a smaller piece (see _d_, Fig. 6); then the inner bulb by similar method. It is now necessary to introduce the smaller bulb into the larger, and for this purpose the larger bulb must be cut into halves. A small but deep cut is made with the file or glass-blowers' knife in the middle of the larger bulb, and at right angles to the axis of the tube on which it is blown. A minute bead of intensely heated glass is now brought in contact with the cut in order to start a crack. This crack may now be led round the bulb as described on page 30. If the work is carried out with care, it is possible to obtain the bulb in two halves as shown by _d_, and these two halves will correspond so exactly that when the cut edges are placed in contact they will be almost air-tight. The two tubes from the smaller bulb should be cut to such a length that they will just rest inside the larger, and the ends should be expanded. Place the inner bulb in position and fit the two halves of the outer bulb together, taking great care not to chip the edges. If the length of the tubes on the inner bulb has been adjusted properly, the inner bulb will be supported in position by their contact with the tubes on the outer bulb. Now rotate the cracked portion of the outer bulb in front of a blowpipe flame and press the halves together very gently as the glass softens. Expand slightly by blowing if necessary. If a small pin-hole develops at the joint it is sometimes possible to close this with a bead of hot glass; but if the bulb has been cut properly there should be no pin-holes formed. The condenser is finished by joining on the side tubes and sealing the inner tube through by the methods already given. In order to blow bulbs large enough to make a useful condenser, it will be convenient to employ the multiple-jet blowpipe described on page 4. _A Soxhlet-Tube or Extraction Apparatus._--This involves the construction of a re-entrant join where the syphon flows into the lower tube. It is of considerable value as an exercise and the complete apparatus is easy to make. A large tube is sealed at the bottom and the top is lipped, as in making a test-tube. A smaller tube is then joined on by a method similar to that given on pag
PREV.   NEXT  
|<   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33   34   35   36   37   38   39   40   41  
42   43   44   45   46   47   48   49   50   51   52   53   >>  



Top keywords:
halves
 

larger

 

smaller

 

contact

 

condenser

 

method

 
length
 
position
 
properly
 

similar


blowpipe

 

involves

 

sealing

 
softens
 

methods

 

gently

 

finished

 

develops

 

slightly

 

joining


blowing

 

formed

 

Expand

 

exercise

 
complete
 

apparatus

 

considerable

 

sealed

 
joined
 

making


lipped

 

bottom

 
syphon
 

employ

 
multiple
 

convenient

 

Soxhlet

 

entrant

 
construction
 

Apparatus


Extraction
 
correspond
 

blowers

 

middle

 

angles

 

brought

 
heated
 

intensely

 

minute

 

purpose