FREE BOOKS

Author's List




PREV.   NEXT  
|<   63   64   65   66   67   68   69   70   71   72   73   74   75   76   77   78   79   80   81   82   83   84   85   86   87  
88   89   90   91   92   93   94   95   96   97   98   99   >>  
ly becomes much concentrated, and it requires high heat and careful management to finish the solution of the bullion. Bars containing more than about 10 per cent. of copper cannot be dissolved at all, owing to the separation of copper sulphate insoluble in the small amount of free acid finally remaining. The advantage gained by dissolving bullion with abundance of free acid in the improved process is so evident that it merely requires to be pointed out. For bullion containing 20 per cent. of copper the author employs six parts of acid to one of bullion; for baser metal still more acid, and so on, never losing more than the stochiometrical percentage of acid and recovering the remainder. In this description he, however, confines himself to the treatment of ordinary silver ore with less than 10 per cent. of copper. In the diagram A A represent two refining pots, 4 ft. in diameter and 3 ft. in depth, each capable of dissolving at one operation as much as 400 pounds of bullion. The acid is stored in the cast iron reservoir, B, which is placed on a level sufficiently high to charge into A by gravitation, and is composed of fresh concentrated acid mixed with the somewhat dilute acid regained from a previous operation. After the bullion is fully dissolved all the acid still available is run from B into A A. The temperature and strength are thereby reduced, the fuming ceases, any still undissolved copper sulphate dissolves, and the gold settles. In assuming that the settling of the gold takes place in A itself, the author follows the practice of the United States mints. In private refineries, where refining is carried on continuously, the settling may take place in an intermediate vessel, and A A be at once recharged. Owing to the large amount of free acid present, the temperature must fall considerably before the separation of silver sulphate commences, and sufficient time may be allowed for settling if the intermediate vessel be judiciously arranged. [Illustration] _Separating the Silver Sulphate._--The clarified solution is siphoned off the gold from A A into C, which is an open cast iron pan, say 8 ft. by 4 ft. and 1 ft. deep. It is supported by means of a flange in another larger pan--not shown in the diagram--into which water may be admitted for cooling. Steam is blown into the acid solution, still very hot, as soon as C is filled. The steam is introduced about 1 in. below the surface of the liquid, blowing perpend
PREV.   NEXT  
|<   63   64   65   66   67   68   69   70   71   72   73   74   75   76   77   78   79   80   81   82   83   84   85   86   87  
88   89   90   91   92   93   94   95   96   97   98   99   >>  



Top keywords:
bullion
 

copper

 

sulphate

 

solution

 

settling

 
intermediate
 

author

 

vessel

 

temperature

 

operation


refining

 

silver

 

diagram

 

dissolved

 
amount
 

requires

 

concentrated

 
dissolving
 
separation
 

recharged


surface
 

liquid

 
perpend
 

blowing

 

considerably

 

introduced

 

present

 

continuously

 

careful

 

assuming


management

 
settles
 
practice
 

refineries

 

carried

 

private

 

United

 

States

 

commences

 

filled


supported

 

flange

 

larger

 

cooling

 
admitted
 

judiciously

 

arranged

 
dissolves
 
allowed
 

sufficient